Contact an Account ManagerExtraction of veterinary drug enrofloxacine from percolate water
Summary
Type: SPE
Application #: 305762
Detection:
Conditions: Column conditioning: 5 mL methanol
Sample aspiration: 100 mL or 1000 mL of pretreated samples were passed through the column by vacuum
Drying: nitrogen
Elution: 4 mL acetonitrile + 1 % formic acid, then 4 mL methanol + 1 % formic acid
Evaporation: to dryness with nitrogen
Reconstitution: 1 mL of 1 mol/L citrate buffer – methanol (1:10, v/v)
Centrifugation: 30000 g; supernantant was determined by LC-MS
Authors: Weiß, K.
Source: Bayerisches Landesamt für Umwelt, Augsburg
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